PARTICLE COUNTER FOR DETERMINING PURITY OF HYDRAULIC FLUID

Revision Date: 9/01
Process Code: Navy/Marines: ID-14-04; Air Force: LA01; Army:LOP
Usage: Navy: High; Marines: High; Army: High; Air Force: High
Compliance Impact: Medium
Alternative for: The Patch Test (Filtration Testing) and its use of  ODSs for Testing Hydraulic Fluids
Applicable EPCRA Targeted Constituents: Freon 113 (CAS: 76-13-1), 1,1,1-Trichloroethane (CAS: 71-55-6)

Overview: A particle counter tests hydraulic fluid quantitatively for contamination by shining a laser through a set quantity of the fluid and counting quantity and size of particles using a photo-detector. The particle counter is a highly effective, accurate, proven electronic technology.

Hydraulic fluid contamination testing for foreign particles or worn metal has traditionally been conducted using the patch test with CFC-113 (a Class 1 Ozone Depleting Substance [ODS] the use of which is no longer allowed), Methyl Chloroform (Class 1 ODS), or Petroleum Solvent, as defined by federal specification PD-680 Type II. The patch test is a three-step process whereby hydraulic fluid is filtered using either a patch or filter, quick-dried using an evaporating agent, and subsequently read by a trained operator. A particle counter is superior for two reasons. First, it eliminates the use of the drying agent (ODS or solvent). Second, it takes the subjectivity out of the process and hence is a more consistent and accurate analytical method as compared to the patch test.

Elimination of ODSs leaves PD-680 Type II as the only approved solvent for use in patch tests. While PD-680 Type II offers a satisfactory alternative, it is not an ideal solution. Problems associated with using PD-680 Type II include increased drying time, use of inaccurate color standards, and subjective interpretation of those standards. The end result is a less accurate, less convenient, and more time-consuming testing procedure for hydraulic fluid contamination.

The use of an electronic particle counter offers a viable alternative to the patch test and produces a more accurate result. This equipment requires no hazardous solvents, and test results are accurate and non-subjective. Use of this technology is approved for Naval activities in the NAVAIR 01-1A-17 Hydraulic Manual.

Through a Navy-funded effort to eliminate ODSs, in conjunction with the Navy's Reverse Engineering Program (a hands-on effort to help field activities deal with rapidly changing environmental regulations), particle counters have been introduced to four prototype sites to completely eliminate the need for CFC-113 in patch tests.

The goals of the hydraulic fluid contamination-testing project were to eliminate the need for ODSs and reduce the need for a patch test. Subtasks of the project included reviewing the sampling frequency requirements, evaluating field replacements for the patch test, investigating alternate solvents, and prototyping, at field level, the most promising candidates. 


Electronic particle counting has long been approved as a means of determining contamination of hydraulic systems, but has been mainly used as a depot maintenance level practice due to the cost and complexity of the particle counter equipment. Bench-top and portable particle counting equipment was evaluated with the goal of finding an inexpensive portable unit suitable for deployment. After investigation, it was determined that none of the portable units were developed enough for prototype at field activities. Although rather costly, the HIAC Model 8011 or 8003 with the ASAP sampler benchtop particle counter appeared to be the best alternative. After a successful two-week initial prototype aboard the USS Theodore Roosevelt, four of the units (8011) were procured for prototype at four sites (NAS Miramar, NAS Cecil Field, NAS Oceana, and USS Theodore Roosevelt), at a total cost of $71,000.

After several months in the prototype stage, the results have been extremely positive. The sample turnaround time has proven to be well within requirements to maintain fleet readiness. The relationship between patch test results and particle counter results has been acceptable. The mechanics using the particle counter equipment are satisfied with its operation and prefer it use to the patch test. The USS Theodore Roosevelt completed the transition to use of the particle counter during their 6-month, 1993 cruise.


Compliance Benefit: The use of a particle counter in place of an ODS will help facilities meet the requirements under 40 CFR 82, Subpart D and Executive Order 12843 requiring federal agencies to maximize the use of safe alternatives to Class I and Class II ozone depleting substances, to the maximum extent practicable. In addition, a particle counter may also reduce the amount of solvents used on site that may decrease the amount of hazardous waste generated. The decrease in hazardous waste helps facilities meet the requirements of waste reduction under RCRA, 40 CFR 262, Appendix, and may also help facilities reduce both their generator status and the number of applicable requirements (i.e., recordkeeping, reporting, inspections, transportation, accumulation time, emergency prevention and preparedness, emergency response) under RCRA, 40 CFR 262. The decrease in solvent and/or ODS use on site will also decrease the possibility that a facility will meet reporting thresholds for those chemicals under 40 CFR 355 and EO 12856.

The compliance benefits listed here are only meant to be used as a general guideline and are not meant to be strictly interpreted. Actual compliance benefits will vary depending on the factors involved, e.g. the amount of workload involved.


Materials
Compatibility:

There are no materials compatibility issues raised by the use of electronic particle counters.


 
Safety and Health: Electronic particle counters require no special health and safety precautions, although mild dermal and eye irritation effects can result from contact with hydraulic fluids. Personal protective equipment should be used. Consult your local industrial health specialist, your local health and safety personnel, and the appropriate MSDS prior to implementing this technology.


Benefits:
  • Removes any subjectivity associated with  the patch test.
  • Eliminates the use of ODSs or solvents.
  • Viable alternative to the patch test.
  • Technology has been in use for over 20 years.
  • Particle counters count both number and size of particles providing quantitative results, thus providing a more accurate reading.
  • More accurate testing may extend vehicle life.


Disadvantages:
  • Routine calibration of units must be maintained to ensure valid results.
  • Glassware used must be extremely clean.
  • High cost of units.
  • Portable units still in development.


Economic Analysis: The following cost elements are for electronic particle counters for determining purity of hydraulic fluid. The economic analysis presented below is for a comparison of a typical patch test employing PD-680 solvent versus the particle counter method. However, this cost analysis would be applicable independent of the solvent employed in the patch test. This analysis is based on Preproduction Initiative NELP performed at NAS North Island and NS Mayport.

Assumptions:

  • Labor rate to operate particle counters (PC) and run Patch Test (PT): $10.39/hr.
  • Tests per year: 660
  • Time to run tests: PC - 8.5 minutes/test; PT - 1 hour/test
  • Milliliters of P-D-680 Type II used per test: 115
  • Cost per milliliter: $0.000685
  • Cost of P-D-680 Type II per test: $0.08
  • Number of filters used per test: 1 filter
  • Cost per filter: $0.56
  • Number of Petri slides used per test: 1
  • Cost per Petri slide: $0.19
  • Total cost per test: $0.83
  • Milliliters of waste generated per test: 230
  • Gallons of waste generated per year: 40
  • Pounds per gallon: 6.5 (estimated)
  • Disposal cost per pound: $2.10
  • PC generates 20 gallons of hydraulic fluid waste per year that is recycled at no cost.
  • Energy for PC and PT: negligible
  • Cost of printer paper and supplies: $422.4
  • Equipment costs: $7,500
  • Particle counter system maintenance cost: $116.25

Annual Operating Cost Comparison for Operating Particle Counter vs. Patch Test

Particle Counter Patch Test
Operational Costs
Labor: $970.20 $6,857
Material: $422.40 $547.80
Energy: $0 $0
Waste Disposal: $0 $546
System Maintenance: $116.55 $0
Total Operational Costs: $1,509 $7,951
Total Recovered Income: $0 $0
Net Annual Cost/Benefit -$1,509 -$7,951



Economic Analysis Summary

Annual Savings for Particle Counter: $6,442
Capital Cost for Diversion Equipment/Process: $7,500
Payback Period for Investment in Equipment/Process: 1.2 years

Click Here to view an Active Spreadsheet for this Economic Analysis and Enter Your Own Values. To return from the Active Spreadsheet, click the reverse arrow in the Tool Bar.


Approving Authority: Approval is controlled locally and should be implemented only after engineering approval has been granted. Major claimant approval is not required.  USAF activities must follow their governing technical orders for determining whether the use of particle counters are appropriate for their application.


NSN/MSDS:
Product NSN Unit Size Cost MSDS*
Particle Counter 6635-01-041-5643 ea. $ 4,008.00  
Particle Counter 6640-01-263-6618 ea. $18,967.10  
Metal Part. Detector 2995-01-433-4830 ea. $ 8,220.00  


*There are multiple MSDSs for most NSNs.
The MSDS (if shown above) is only meant to serve as an example.



 

Points of Contact: Air Force:
Mr. Leo Broome
Detachment 3, WR-ALC/AFTT
Bldg. 1621-K
2261 Hughes Avenue, Suite 123
Lackland, AFB, TX  78236-9823
Phone: (210) 925-7613
DSN: 945-7613
FAX: (210) 925-9964
Email:  leopold.broome@lackland.af.mil

Ms. Lois Gschwender
AFRL/MLBT
2941 P St., Building 654, Room 136
WPAFB, OH 45433-7750
Phone: (937) 255-7530
DSN: 785-7530
FAX: (937) 255-2176
Email:  lois.gschwender@wpafb.af.mil


Vendors: This is not meant to be a complete list, as there may be other suppliers of this type of equipment.

Pacific Scientific Instruments (High Yield Technology)
481 California Ave.
Grants Pass, OR 97526
Phone: (800) 866-7889
or (541) 472-6515
FAX: (541) 479-3057
Contact:  John Early
URL:  http://www.particle.com/

Climet Instruments Company
1320 W. Colton Avenue
Redlands, CA  92374
Phone:  (909) 793-2788
FAX:  (909) 793-1738|
URL:  http://www.climet.com/


Sources: Mr. Leo Broome, San Antonio Air Logistics Center, January 1999.
Mr. Glen Fisher, HIAC/ROYCO, May 1996
Mr. Mike Patterson, Mensco, May 1996
Mr. Mike Gibson, Naval Aviation Depot-Cherry Point, May 1996
Mr. Michele Guerard, Millipore, June 1996
Mr. Grant Moscowitz, Ecolink, June 1996
P2 Equipment Book, Office of the Chief of Naval Operations, May 1997

 


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