Pollution Prevention Case Study

The Falk Corporation

Substitution of oil quench with water-polymer solution
in heat-treat pit carburizing operations

Standard Industrial Classification (SIC) Speed changers, drives and gears/3566
Type of Waste Mineral oil liquid
Strategy Material substitution and process modification
Company Background The Falk Corporation was established in the Greater Milwaukee Area in 1892 and presently has approximately 1,300 employees at its main plant. Falk produces mechanical power transmission equipment and sells the products worldwide. Products include custom engineered steel castings, enclosed gear drives, open gearing, custom industrial drives, and shaft fluid couplings. Industries served include: cement, mining, automotive, paper, construction, and marine.
Original Process This case study applies to Falk's pit carburizing of pinions and gears. Quench oil was used to heat-treat (harden) both open-fired and special-atmosphere (carburized) parts in Falk's heat-treat department. Parts are quenched at a temperature of 1525° F.
Motivation State regulations require that any new process line emitting greater than 3.1 pounds of volatile organic compounds (VOC's)/hour use a capture device with an 85 percent efficiency. For Falk, this device would have required a capital investment of $500,000 to $1,000,000 plus associated energy and maintenance costs. The company sought to avoid these costs and also wanted to reduce drag-out in the quench tank. Falk was also concerned about possible smoke and fire hazards associated with oil quenching of large parts.
Pollution Prevention Process The pit quench system is a recirculatory system that holds 45,000 gallons of quench media. Pumps circulate the media from a surge tank (20,000 gallon) to the main quench tank (25,000 gallon). Heating and cooling systems are integrated into the process. During a parts quench, agitators circulate the media within the quench tank. The equipment has a maximum capacity of 15 tons, resulting in maximum emissions from the system of 2.17 pounds VOC/per hour which is below the maximum allowable 3.1 pounds VOC/per hour limit. The polymer exhibits virtually no drag-out when removing the parts from the quench tank. Any residual polymer clinging to the quenched part is simply rinsed back into the quench tank with a brief water spray. This system reduces another waste stream (tramp oil at the parts washer) while also reducing costs for purchase of raw material.
Stage of Development The system is in full use in Falk's pit carburizing facility
Level of Commercialization Polymer quenchant, which is mixed with water at a ratio of approximately one part polymer to five parts water, has been commercially available for many years. This is the first time that it has been applied to a system this large.
Material/Energy Balance Proposed Pollution Control Process
Feedstock
100 percent quench oil

Waste
VOC air emissions and waste oil

Disposal
Wastewater (disposed of offsite by a Waste Management Company).

Pollution Prevention Process
Feedstock
80 percent H2O (fresh city water)
20 percent polymer

Waste
VOC air emissions are ~0.144 pounds per ton of steel quenched.

Disposal
None. This is a closed loop system.

Economics Capital Costs
Polymer quench system
7,000 gallons of polymer
Misc. fixtures, lifting devices
Emergency storage tank
$420,000
$200,000
$ 20,000
$ 20,000
$660,000

Operation/Maintenance Costs
Not available.

Payback Period
Not calculated. However, the company avoided control equipment and maintenance costs associated with the proposed process. This has resulted in a cost avoidance of ~$542,000.

Benefits The polymer quenchant, when mixed with water, costs about the same per gallon as the oil quenchant. VOC's are reduced to a fraction of that with oil, and drag-out is virtually eliminated. In over a year of operation, no new raw product has been added to the system.
Obstacles Until now, polymer quenchant had not been applied to finished carburized gear parts this large. The greatest risk was that parts would crack due to the cooling rate of the quenchant. Falk experimented and found that with the proper concentration and the proper start temperature the cooling curves were similar to oil quenching. Additional features were designed into the system to reduce the risk of cracking.
Technology Transfer This process has the potential for use in other heat treating application systems.
Company Address The Falk Corporation
3001 West Canal Street
P.O. Box 492
Milwaukee, Wisconsin 53201-0492
Contact Person Jack G. Habrat, P.E.
Plant Engineer
414/342-3131
Pollution Prevention Resources Free, On-site Technical Assistance
University of Wisconsin Extension
Solid and Hazardous Waste Education Center
Milwaukee area: 414/475-2845
Remainder of state: 608/262-0385

Pollution Prevention Information Clearinghouse
Wisconsin Department of Natural Resources
Hazardous Waste Minimization Program
608/264-8852, 608/267-9523 or 608/267-3763

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Bureau of Cooperative Environmental Assistance
Wisconsin Department of Natural Resources
P.O. Box 7921
Madison, WI   53707
608/267-9700

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